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5.32 Intermediate Chemical Experimentation (MIT) 5.32 Intermediate Chemical Experimentation (MIT)

Description

5.32 involves more advanced experimental work than 5.310 or 5.311. The course emphasizes organic synthesis assisted by chiral catalysis, purification, and analysis of organic compounds employing such methods as IR, 1D and 2D NMR, UV spectroscopies and mass spectrometry, and thin layer and non-chiral and chiral gas chromatography. In 5.32, experiments also involve enzyme purification, characterization and assays, as well as molecular modeling in organic synthesis and in biochemical systems. WARNING NOTICE The experiments described in these materials are potentially hazardous and require a high level of safety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such 5.32 involves more advanced experimental work than 5.310 or 5.311. The course emphasizes organic synthesis assisted by chiral catalysis, purification, and analysis of organic compounds employing such methods as IR, 1D and 2D NMR, UV spectroscopies and mass spectrometry, and thin layer and non-chiral and chiral gas chromatography. In 5.32, experiments also involve enzyme purification, characterization and assays, as well as molecular modeling in organic synthesis and in biochemical systems. WARNING NOTICE The experiments described in these materials are potentially hazardous and require a high level of safety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such

Subjects

intermediate chemical experimentation | intermediate chemical experimentation | experiment | experiment | chemistry | chemistry | organic synthesis | organic synthesis | chiral catalysis | chiral catalysis | purification | purification | organic chemistry | organic chemistry | laboratory | laboratory | IR | IR | 1D NMR | 1D NMR | 2D NMR | 2D NMR | UV spectroscopy | UV spectroscopy | mass spectrometry | mass spectrometry | thin layer gas chromatography | thin layer gas chromatography | non-chiral gas chromatography | non-chiral gas chromatography | chiral gas chromatography | chiral gas chromatography | enzyme purification | enzyme purification | characterization | characterization | assays | assays | molecular modeling | molecular modeling | biochemical systems | biochemical systems

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see http://ocw.mit.edu/terms/index.htm

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5.32 Intermediate Chemical Experimentation (MIT)

Description

5.32 involves more advanced experimental work than 5.310 or 5.311. The course emphasizes organic synthesis assisted by chiral catalysis, purification, and analysis of organic compounds employing such methods as IR, 1D and 2D NMR, UV spectroscopies and mass spectrometry, and thin layer and non-chiral and chiral gas chromatography. In 5.32, experiments also involve enzyme purification, characterization and assays, as well as molecular modeling in organic synthesis and in biochemical systems. WARNING NOTICE The experiments described in these materials are potentially hazardous and require a high level of safety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such

Subjects

intermediate chemical experimentation | experiment | chemistry | organic synthesis | chiral catalysis | purification | organic chemistry | laboratory | IR | 1D NMR | 2D NMR | UV spectroscopy | mass spectrometry | thin layer gas chromatography | non-chiral gas chromatography | chiral gas chromatography | enzyme purification | characterization | assays | molecular modeling | biochemical systems

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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5.32 Intermediate Chemical Experimentation (MIT)

Description

5.32 involves more advanced experimental work than 5.310 or 5.311. The course emphasizes organic synthesis assisted by chiral catalysis, purification, and analysis of organic compounds employing such methods as IR, 1D and 2D NMR, UV spectroscopies and mass spectrometry, and thin layer and non-chiral and chiral gas chromatography. In 5.32, experiments also involve enzyme purification, characterization and assays, as well as molecular modeling in organic synthesis and in biochemical systems. WARNING NOTICE The experiments described in these materials are potentially hazardous and require a high level of safety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such

Subjects

intermediate chemical experimentation | experiment | chemistry | organic synthesis | chiral catalysis | purification | organic chemistry | laboratory | IR | 1D NMR | 2D NMR | UV spectroscopy | mass spectrometry | thin layer gas chromatography | non-chiral gas chromatography | chiral gas chromatography | enzyme purification | characterization | assays | molecular modeling | biochemical systems

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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5.301 Chemistry Laboratory Techniques (MIT) 5.301 Chemistry Laboratory Techniques (MIT)

Description

This course is an intensive introduction to the techniques of experimental chemistry and gives first year students an opportunity to learn and master the basic chemistry lab techniques for carrying out experiments. Students who successfully complete the course and obtain a "Competent Chemist" (CC) or "Expert Experimentalist" (EE) rating are likely to secure opportunities for research work in a chemistry lab at MIT. Acknowledgements The laboratory manual and materials for this course were prepared by Dr. Katherine J. Franz and Dr. Kevin M. Shea with the assistance of Professors Rick L. Danheiser and Timothy M. Swager. Materials have been revised by Dr. J. Haseltine, Dr. Kevin M. Shea, and Dr. Sarah A. Tabacco. WARNING NOTICE The experiments described in these materials a This course is an intensive introduction to the techniques of experimental chemistry and gives first year students an opportunity to learn and master the basic chemistry lab techniques for carrying out experiments. Students who successfully complete the course and obtain a "Competent Chemist" (CC) or "Expert Experimentalist" (EE) rating are likely to secure opportunities for research work in a chemistry lab at MIT. Acknowledgements The laboratory manual and materials for this course were prepared by Dr. Katherine J. Franz and Dr. Kevin M. Shea with the assistance of Professors Rick L. Danheiser and Timothy M. Swager. Materials have been revised by Dr. J. Haseltine, Dr. Kevin M. Shea, and Dr. Sarah A. Tabacco. WARNING NOTICE The experiments described in these materials a

Subjects

chemistry | chemistry | experiment | experiment | laboratory techniques | laboratory techniques | purification | purification | transfer and extraction | transfer and extraction | column chromatography | column chromatography | protein assays | protein assays | error analysis | error analysis | NMR | NMR | IR | IR | gas chromatography | gas chromatography | spectroscopy | spectroscopy | UV-Vis | UV-Vis | experimental chemistry | experimental chemistry | original research projects | original research projects

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see http://ocw.mit.edu/terms/index.htm

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5.301 Chemistry Laboratory Techniques (MIT) 5.301 Chemistry Laboratory Techniques (MIT)

Description

This course is an intensive introduction to the techniques of experimental chemistry and gives first year students an opportunity to learn and master the basic chemistry lab techniques for carrying out experiments. Students who successfully complete the course and obtain a "Competent Chemist" (CC) or "Expert Experimentalist" (EE) rating are likely to secure opportunities for research work in a chemistry lab at MIT. Acknowledgements The laboratory manual and materials for this course were prepared by Dr. Katherine J. Franz and Dr. Kevin M. Shea with the assistance of Professors Rick L. Danheiser and Timothy M. Swager. Materials have been revised by Dr. J. Haseltine, Dr. Kevin M. Shea, Dr. Sarah A. Tabacco, Dr. Kimberly L. Berkowski, Anne M. (Gorham) Rachupka, and Dr. Joh This course is an intensive introduction to the techniques of experimental chemistry and gives first year students an opportunity to learn and master the basic chemistry lab techniques for carrying out experiments. Students who successfully complete the course and obtain a "Competent Chemist" (CC) or "Expert Experimentalist" (EE) rating are likely to secure opportunities for research work in a chemistry lab at MIT. Acknowledgements The laboratory manual and materials for this course were prepared by Dr. Katherine J. Franz and Dr. Kevin M. Shea with the assistance of Professors Rick L. Danheiser and Timothy M. Swager. Materials have been revised by Dr. J. Haseltine, Dr. Kevin M. Shea, Dr. Sarah A. Tabacco, Dr. Kimberly L. Berkowski, Anne M. (Gorham) Rachupka, and Dr. Joh

Subjects

chemistry | chemistry | experiment | experiment | laboratory techniques | laboratory techniques | purification | purification | transfer and extraction | transfer and extraction | column chromatography | column chromatography | protein assays | protein assays | error analysis | error analysis | NMR | NMR | IR | IR | gas chromatography | gas chromatography | spectroscopy | spectroscopy | UV-Vis | UV-Vis

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see http://ocw.mit.edu/terms/index.htm

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5.37 Introduction to Organic Synthesis Laboratory (MIT) 5.37 Introduction to Organic Synthesis Laboratory (MIT)

Description

This course, which spans a third of a semester, provides students with experience using techniques employed in synthetic organic chemistry. It also introduces them to the exciting research area of catalytic chiral catalysis. This class is part of the new laboratory curriculum in the MIT Department of Chemistry. Undergraduate Research-Inspired Experimental Chemistry Alternatives (URIECA) introduces students to cutting edge research topics in a modular format. This course, which spans a third of a semester, provides students with experience using techniques employed in synthetic organic chemistry. It also introduces them to the exciting research area of catalytic chiral catalysis. This class is part of the new laboratory curriculum in the MIT Department of Chemistry. Undergraduate Research-Inspired Experimental Chemistry Alternatives (URIECA) introduces students to cutting edge research topics in a modular format.

Subjects

experiment | experiment | laboratory | laboratory | organic | organic | synthesis | synthesis | chemistry | chemistry | diels-alder | diels-alder | catalysis | catalysis | asymmetric | asymmetric | cycloaddition | cycloaddition | enantioselectivity | enantioselectivity | diastereoselectivity | diastereoselectivity | chirality | chirality | chiral gas chromatography | chiral gas chromatography | stereochemistry | stereochemistry | convergent strategies | convergent strategies | retrosynthetic analysis | retrosynthetic analysis

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see http://ocw.mit.edu/terms/index.htm

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5.310 Laboratory Chemistry (MIT) 5.310 Laboratory Chemistry (MIT)

Description

Laboratory Chemistry (5.310) introduces experimental chemistry for students requiring a chemistry laboratory who are not majoring in chemistry. Students must have completed general chemistry (5.111) and have completed or be concurrently enrolled in the first semester of organic chemistry (5.12). The course covers principles and applications of chemical laboratory techniques, including preparation and analysis of chemical materials, measurement of pH, gas and liquid chromatography, visible-ultraviolet spectrophotometry, infrared spectroscopy, kinetics, data analysis, and elementary synthesis. NOTE: The Staff for this course would like to acknowledge that the experiments include contributions from past instructors, course textbooks, and others affiliated with course #5.310. Since the Laboratory Chemistry (5.310) introduces experimental chemistry for students requiring a chemistry laboratory who are not majoring in chemistry. Students must have completed general chemistry (5.111) and have completed or be concurrently enrolled in the first semester of organic chemistry (5.12). The course covers principles and applications of chemical laboratory techniques, including preparation and analysis of chemical materials, measurement of pH, gas and liquid chromatography, visible-ultraviolet spectrophotometry, infrared spectroscopy, kinetics, data analysis, and elementary synthesis. NOTE: The Staff for this course would like to acknowledge that the experiments include contributions from past instructors, course textbooks, and others affiliated with course #5.310. Since the

Subjects

lab | lab | chemistry | chemistry | laboratory | laboratory | experiment | experiment | pH | pH | gas chromatography | gas chromatography | liquid chromatography | liquid chromatography | visible-ultraviolet spectrophotometry | visible-ultraviolet spectrophotometry | infrared spectroscopy | infrared spectroscopy | kinetics | kinetics | data analysis | data analysis | elementary synthesis | elementary synthesis | amino acid | amino acid | ferrocene | ferrocene | essential oil | essential oil | potentiometric titration | potentiometric titration | techniques | techniques | measurement | measurement | materials | materials | data | data | analysis | analysis | elementary | elementary | synthesis | synthesis | amino | amino | acid | acid | essential | essential | oil | oil | gas | gas | chromatography | chromatography | infrared | infrared | spectroscopy | spectroscopy | liquid | liquid | potentiometric | potentiometric | titration | titration | visible | visible | ultraviolet | ultraviolet | spectrophotometry | spectrophotometry

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see http://ocw.mit.edu/terms/index.htm

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5.310 Laboratory Chemistry (MIT)

Description

Laboratory Chemistry (5.310) introduces experimental chemistry for students requiring a chemistry laboratory who are not majoring in chemistry. Students must have completed general chemistry (5.111) and have completed or be concurrently enrolled in the first semester of organic chemistry (5.12). The course covers principles and applications of chemical laboratory techniques, including preparation and analysis of chemical materials, measurement of pH, gas and liquid chromatography, visible-ultraviolet spectrophotometry, infrared spectroscopy, kinetics, data analysis, and elementary synthesis. NOTE: The Staff for this course would like to acknowledge that the experiments include contributions from past instructors, course textbooks, and others affiliated with course #5.310. Since the

Subjects

lab | chemistry | laboratory | experiment | pH | gas chromatography | liquid chromatography | visible-ultraviolet spectrophotometry | infrared spectroscopy | kinetics | data analysis | elementary synthesis | amino acid | ferrocene | essential oil | potentiometric titration | techniques | measurement | materials | data | analysis | elementary | synthesis | amino | acid | essential | oil | gas | chromatography | infrared | spectroscopy | liquid | potentiometric | titration | visible | ultraviolet | spectrophotometry

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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Laboratory Investigation of Chewing Gum

Description

A laboratory-based investigation into the chemical flavourings found in chewing gum. The investigation is based around some 'problem' gum and the students are set the challenge of solving the problem. Students contribute to experimental design and carry out extractions, purifications and analysis of purified extracts by GC and/or GC-MS.

Subjects

chewing gum | chemistry | flavourings | problem solving | laboratory | extractions | gas chromatography | mass spectrometry | ukoer | sfsoer | Physical sciences | F000

License

Attribution-Noncommercial-Share Alike 2.0 UK: England & Wales Attribution-Noncommercial-Share Alike 2.0 UK: England & Wales http://creativecommons.org/licenses/by-nc-sa/2.0/uk/ http://creativecommons.org/licenses/by-nc-sa/2.0/uk/

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Laboratory Investigation of Fatty Acid Supplements

Description

This is a laboratory-based investigation of so-called essential fatty acids (e.g. omega-3,6 fatty acids) in supplements. Students carry out extractions and analyse extracts by GC and/or GC/MS. They also carry out small scale derivatisation reactions and purifications. Data is analaysed wuth respect to composition of individual supplements, comparison with packaging information, etc.

Subjects

chemistry | laboratory | fatty acids | food | analytical | gas chromatography | mass spectrometry | sfsoer | ukoer | Physical sciences | F000

License

Attribution-Noncommercial-Share Alike 2.0 UK: England & Wales Attribution-Noncommercial-Share Alike 2.0 UK: England & Wales http://creativecommons.org/licenses/by-nc-sa/2.0/uk/ http://creativecommons.org/licenses/by-nc-sa/2.0/uk/

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Laboratory Investigation of Parabens

Description

This is a laboratory-based investigation of preservative chemicals commonly found in household products - parabens. Students carry out extractions of parabens froma product of choice and analyse the extracts using either GC or HPLC. Suggested methods are given for each analytical method. Composition data are compared against EU legislation for the use of parabens

Subjects

chemistry | analytical | parabens | gas chromatography | hplc | eu | Physical sciences | F000

License

Attribution-Noncommercial-Share Alike 2.0 UK: England & Wales Attribution-Noncommercial-Share Alike 2.0 UK: England & Wales http://creativecommons.org/licenses/by-nc-sa/2.0/uk/ http://creativecommons.org/licenses/by-nc-sa/2.0/uk/

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Analytical Science

Description

Wales undergraduate level and as a CPD training resource

Subjects

ukoer | sfsoer | oer | open educational resources | metadata | analytical science | cpd training resource | analytical chemistry | measurement science | analytical process model | skills for analytical science | skills for analytical chemistry | analytical sample preparation | separation and concentration of analytes | units of measurement | volumetric techniques | gravimetric techniques | calibration methods | standard-addition | method of internal-standards | statistical analysis of data | measurement uncertainty | chromatographic methods | thin layer chromatography | gc | gas chromatography | hplc | high-performance liquid chromatography | capillary electrophoresis | potentiometry | ion-selective electrodes | amperometry | coulometry | plated film thickness | electromagnetic spectrum | electronic transitions | vibrational energy | comparison of spectroscopic techniques | fluorescence spectroscopy | mid infra-red spectroscopy | near infra-red spectroscopy | aas | atomic absorption spectroscopy | atomic emission spectroscopy | inductively coupled plasme emission spectroscopy | icpms | icpes | atomic fluorescence spectroscopy | comparison of elemental analysis techniques | principles of mass spectroscopy | electron impact mass spectroscopy | chemical ionisation mass spectroscopy | quadrupole mass spectroscopy | time-of-flight mass analysers | ion-trap mass analysers | off-line sampling systems | at-line sampling systems | on-line sampling systems | in-line sampling systems | performance characteristics of analytical techniques | flow injection analysis | fia | process gc | process ir | process ms | process uv/visible | quality management | quality assurance | qa | vam principles | quality control | qc | analytical method validation | analytical method performance characteristics | sampling of solids | liquids and gases | measurement of ph | karl fischer titration | uv/visible spectroscopy | beer's law | beer-lambert law | deviations from beer's law | mid ir spectroscopy | near ir spectroscopy | raman spectroscopy | fourier transform spectroscopies | x-ray methods | x-ray fluorescence spectroscopy | gc-ms | lc-ms | Physical sciences | F000

License

Attribution-Noncommercial-No Derivative Works 2.0 UK: England & Wales Attribution-Noncommercial-No Derivative Works 2.0 UK: England & Wales http://creativecommons.org/licenses/by-nc-nd/2.0/uk/ http://creativecommons.org/licenses/by-nc-nd/2.0/uk/

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5.301 Chemistry Laboratory Techniques (MIT)

Description

This course is an intensive introduction to the techniques of experimental chemistry and gives first year students an opportunity to learn and master the basic chemistry lab techniques for carrying out experiments. Students who successfully complete the course and obtain a "Competent Chemist" (CC) or "Expert Experimentalist" (EE) rating are likely to secure opportunities for research work in a chemistry lab at MIT. Acknowledgements The laboratory manual and materials for this course were prepared by Dr. Katherine J. Franz and Dr. Kevin M. Shea with the assistance of Professors Rick L. Danheiser and Timothy M. Swager. Materials have been revised by Dr. J. Haseltine, Dr. Kevin M. Shea, and Dr. Sarah A. Tabacco. WARNING NOTICE The experiments described in these materials a

Subjects

chemistry | experiment | laboratory techniques | purification | transfer and extraction | column chromatography | protein assays | error analysis | NMR | IR | gas chromatography | spectroscopy | UV-Vis | experimental chemistry | original research projects

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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5.301 Chemistry Laboratory Techniques (MIT)

Description

This course is an intensive introduction to the techniques of experimental chemistry and gives first year students an opportunity to learn and master the basic chemistry lab techniques for carrying out experiments. Students who successfully complete the course and obtain a "Competent Chemist" (CC) or "Expert Experimentalist" (EE) rating are likely to secure opportunities for research work in a chemistry lab at MIT. Acknowledgements The laboratory manual and materials for this course were prepared by Dr. Katherine J. Franz and Dr. Kevin M. Shea with the assistance of Professors Rick L. Danheiser and Timothy M. Swager. Materials have been revised by Dr. J. Haseltine, Dr. Kevin M. Shea, Dr. Sarah A. Tabacco, Dr. Kimberly L. Berkowski, Anne M. (Gorham) Rachupka, and Dr. Joh

Subjects

chemistry | experiment | laboratory techniques | purification | transfer and extraction | column chromatography | protein assays | error analysis | NMR | IR | gas chromatography | spectroscopy | UV-Vis

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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5.37 Introduction to Organic Synthesis Laboratory (MIT)

Description

This course, which spans a third of a semester, provides students with experience using techniques employed in synthetic organic chemistry. It also introduces them to the exciting research area of catalytic chiral catalysis. This class is part of the new laboratory curriculum in the MIT Department of Chemistry. Undergraduate Research-Inspired Experimental Chemistry Alternatives (URIECA) introduces students to cutting edge research topics in a modular format.

Subjects

experiment | laboratory | organic | synthesis | chemistry | diels-alder | catalysis | asymmetric | cycloaddition | enantioselectivity | diastereoselectivity | chirality | chiral gas chromatography | stereochemistry | convergent strategies | retrosynthetic analysis

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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5.310 Laboratory Chemistry (MIT)

Description

Laboratory Chemistry (5.310) introduces experimental chemistry for students requiring a chemistry laboratory who are not majoring in chemistry. Students must have completed general chemistry (5.111) and have completed or be concurrently enrolled in the first semester of organic chemistry (5.12). The course covers principles and applications of chemical laboratory techniques, including preparation and analysis of chemical materials, measurement of pH, gas and liquid chromatography, visible-ultraviolet spectrophotometry, infrared spectroscopy, kinetics, data analysis, and elementary synthesis. NOTE: The Staff for this course would like to acknowledge that the experiments include contributions from past instructors, course textbooks, and others affiliated with course #5.310. Since the

Subjects

lab | chemistry | laboratory | experiment | pH | gas chromatography | liquid chromatography | visible-ultraviolet spectrophotometry | infrared spectroscopy | kinetics | data analysis | elementary synthesis | amino acid | ferrocene | essential oil | potentiometric titration | techniques | measurement | materials | data | analysis | elementary | synthesis | amino | acid | essential | oil | gas | chromatography | infrared | spectroscopy | liquid | potentiometric | titration | visible | ultraviolet | spectrophotometry

License

Content within individual OCW courses is (c) by the individual authors unless otherwise noted. MIT OpenCourseWare materials are licensed by the Massachusetts Institute of Technology under a Creative Commons License (Attribution-NonCommercial-ShareAlike). For further information see https://ocw.mit.edu/terms/index.htm

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